Elsevier

Materials Science and Engineering: A

Volume 644, 17 September 2015, Pages 53-60
Materials Science and Engineering: A

Effect of martensite morphology on low cycle fatigue behaviour of dual phase steels: Experimental and microstructural investigation

https://doi.org/10.1016/j.msea.2015.07.044Get rights and content

Abstract

The low cycle fatigue (LCF) behaviour of a dual phase (DP) steel with different martensite morphologies has been investigated in the present work. DP steels with coarse martensite morphologies show inferior LCF life in comparison with fine martensite morphologies for all martensite volume fractions examined. It is suggested that this is be due to the development of larger local plastic strain concentrations in the ferrite with a coarser microstructure, compared to the finer microstructural morphology. Fatigue cracks were observed to initiate inside ferrite grains, and to preferentially propagate through the softer ferrite phase. The average sub-cell size was finer in samples with higher martensite volume fractions, but the sub-cell size was almost unaffected by the martensite morphology.

Introduction

Low weight car bodies are one of the primary requirements in the automotive industry in order to reduce fuel consumption and emissions. Automobile body weight reduction is possible in two ways: increased utilisation of low density materials such as Al alloys, or the use of high strength formable steels which enable a reduction in the sheet thickness. Advanced high strength steels (AHSS) are a preferred choice, mainly due to the significantly cheaper cost of this material compared to the light alloys [1]. AHSS meet the two main design requirements of the automotive industry: high strength and good formability. Dual phase (DP) steels are the most extensively used AHSS due to their high strength and ductility combination. Other added advantages of DP steels include improved service performances in crashworthiness and fatigue durability [2], [3], make them the current designers choice in automotive applications.

Dual phase (DP) steels consist of hard martensite islands embedded in a soft matrix of ferrite. Such a two phase microstructure is created by intercritical annealing or by controlled cooling after hot rolling. By controlling the intercritical annealing temperature DP steels with different martensite volume fractions can be created. It is well documented in literature that depending upon the martensite volume fraction and morphology, the tensile properties of DP steels can be significantly different, even for the same chemical composition [4–6]. Higher volume fractions of martensite increase the flow stress of the steel, and this is typically accompanied by a decrease in the ductility. Strain partitioning between the soft ferrite and hard martensite phases is reported in literature [5–8], with experimental and physically-based microstructural simulation [8] showing clear strain partitioning between phases. As a consequence of strain partitioning between phases the softer ferrite phase carries a larger amount of the imposed strain, and that this can lead to significant strain localisation. It may be the case too that strain partitioning occurs during low cycle fatigue, and the microstructural evolution during load cycling is therefore an area of great interest for DP steels for structural applications.

The fatigue performance of the materials used for automotive body structures are necessary for design and material selection consideration due to the cyclic loads/strains that are experienced during normal use. The nominal stress level are maintained below the yield stress of the material during the vehicle design, however small plastic deformation can be observed in the presence of stress riser. The bulk material can deform in cyclic elastic manner however, micro cyclic plasticity may be observed in the stress concentrated area. Fatigue cracks are more likely to initiate form those stress concentrated regions where the material may deform in micro cyclic plasticity manner. This makes it important to understand the effects of low-cycle fatigue (LCF) on the performance of automotive materials.

There have been a substantial number of studies examining the monotonic deformation behaviour of DP steels, however, comparatively few studying the low cycle fatigue (LCF) behaviour of this material [5], [6], [7], [9]. Authors previous work [10] reported that the LCF life for a given plastic strain amplitude is significantly reduced by an increase in the martensite volume fraction. It was reported that cyclic hardening occurs during the initial few cycles followed by relatively low cyclic softening [10]. Mediratta et al. [5] also reported cyclic hardening in the initial few cycles, followed by an almost stable response. Zhongguang et al. [11] reported that DP steel with a martensite volume fraction of 50% shows cyclic softening behaviour at high strain amplitudes while cyclic hardening behaviour for lower strain amplitudes. Despite slight differences in the specific behaviour, all published literature on LCF behaviour of DP steel unanimously concluded that the martensite volume fraction has a significant effect on LCF life and cyclic hardening–softening behaviour. The effect of martensite morphology on LCF behaviour of DP steel, however, is less investigated. Mediratta et al. [6] reported that martensite morphology had a significant effect on LCF behaviour of DP steel with a 21% martensite volume fraction. They reported that DP steel with fine uniform dispersion of martensite in a fine grained ferrite matrix shows the best LCF life, while DP steel with coarse martensitic particles encapsulated in a ferrite matrix shows inferior LCF life. This current study will therefore investigate the LCF performance of DP steels with different martensite morphology at a wide range of martensite volume fractions. This investigation will be helpful in understanding the effect of LCF on one of the key elements of a DP steel microstructure, which allows better prediction capabilities of fatigue life and in the design of novel multiphase steel microstructures that show better fatigue performance.

Section snippets

Experimental methodology

A 2 mm thick DP steel sheet with a nominal chemical composition (in wt%) of: C 0.093, Mn 1.93, Si 0.88, P 0.014, Cr 0.022, Al 0.034 and balance Fe was considered for the present investigation. DP steel with two different martensite morphologies at various martensite volume fractions were generated by a three step intercritical annealing process. For heat treatment purpose, 75 mm×150 mm (Rolling×Transverse direction) rectangular sheets were selected. The schematic diagram of heat treatment process

Initial properties

Optical microstructures are shown in Fig. 3 for various heat treatment conditions. All the steels have exactly the same chemical composition. High prolonged holding temperature (1200 °C and one hour) results in a coarse ferrite grain and coarse martensite morphology. Fig. 3(b), (d) and (f) show fine martensite morphologies with martensite volume fractions of 13%, 20% and 49% (hereafter referred to as F_13%, F_20% and F_49%). Coarse martensite morphologies from the higher temperature heat

Effect of morphology on fatigue life

The plastic strain amplitude is recognized to be the key contributor to low cycle fatigue damage [7], [10], [12]. However, LCF tests such as the ones carried out in the present case are typically conducted under constant total strain amplitude control. We note here that the yield strength of the material has significant effect on LCF life under these conditions. Higher yield strength materials produce a larger elastic strain component for a given applied total strain, and hence a smaller

Conclusions

Dual Phase (DP) steels with different martensite morphologies and volume fractions were prepared from a single chemical composition. The following conclusions can be made from the LCF investigation:

  • The cyclic hardening and softening behaviour of DP steels is highly dependent upon martensite volume fraction, while a very weak dependency is observed with martensite morphology. For both fine and coarse martensite morphologies cyclic hardening and softening behaviour alters with martensite volume

Acknowledgement

The present work was funded by the Alfred Deakin Post-Doctoral Fellowship. The present work was carried out with the support of the Deakin Advanced Characterisation Facility. The assistance of Lynton Leigh with the heat treatment work and Rodney Seiffert with the specimen fabrication work are gratefully acknowledged.

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