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Microstructure Evolution and Mechanical Behavior of a CMnSiAl TRIP Steel Subjected to Partial Austenitization Along with Quenching and Partitioning Treatment

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Abstract

The present study investigated the microstructure evolution and mechanical behavior in a low carbon CMnSiAl transformation-induced plasticity (TRIP) steel, which was subjected to a partial austenitization at 1183 K (910 °C) followed by one-step quenching and partitioning (Q&P) treatment at different isothermal holding temperatures of [533 K to 593 K (260 °C to 320 °C)]. This thermal treatment led to the formation of a multi-phase microstructure consisting of ferrite, tempered martensite, bainitic ferrite, fresh martensite, and retained austenite, offering a superior work-hardening behavior compared with the dual-phase microstructure (i.e., ferrite and martensite) formed after partial austenitization followed by water quenching. The carbon enrichment in retained austenite was related to not only the carbon partitioning during the isothermal holding process, but also the carbon enrichment during the partial austenitization and rapid cooling processes, which has broadened our knowledge of carbon partitioning mechanism in conventional Q&P process.

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References

  1. J.G. Speer, D.K. Matlock, B.C. De Cooman, J.G. Schroth: Acta Mater., 2003, vol. 51, pp. 2611-2622.

    Article  Google Scholar 

  2. J.G. Speer, A.M. Streicher, D.K. Matlock, F. Rizzo, G. Krauss: Austenite formation and decomposition, TMS/ISS, Warrendale, PA, 2003, pp. 505-522.

    Google Scholar 

  3. V.F. Zackay, E.R. Parker, D. Fahr, R. Busch: Trans. Am. Soc. Met., 1967, vol. 60, pp. 252-259.

    Google Scholar 

  4. D.V. Edmonds, K. He, F.C. Rizzo, B.C. De Cooman, D.K. Matlock, J.G. Speer: Mater. Sci. Eng. A, 2006, vol. 438, pp. 25-34.

    Article  Google Scholar 

  5. A.J. Clarke: Ph.D. Thesis, Colorado School of Mines, Golden, CO, 2006.

  6. C.Y. Wang, J. Shi, W.Q. Cao, H. Dong: Mater. Sci. Eng. A, 2010, vol. 527, pp. 3442-3449.

    Article  Google Scholar 

  7. M.J. Santofimia, L. Zhao, R. Petrov, C. Kwakernaak, W.G. Sloof, J. Sietsma: Acta Mater., 2011, vol. 59, pp. 6059-6068.

    Article  Google Scholar 

  8. N. Zhong, X. Wang, Y. Rong, L. Wang: J. Mater. Sci. Technol., 2006, vol. 22, pp. 751-754.

    Google Scholar 

  9. D. De Knijf, R. Petrov, C. Föjer, L.A.I. Kestens: Mater. Sci. Eng. A, 2014, vol. 615, pp. 107-115.

    Article  Google Scholar 

  10. X. Tan, Y. Xu, X. Yang, D. Wu: Mater. Sci. Eng. A, 2014, vol. 589, pp. 101-111.

    Article  Google Scholar 

  11. M.J. Santofimia, C. Kwakernaak, W.G. Sloof, L. Zhao, J. Sietsma: Mater. Charact., 2010, vol. 61, pp. 937-942.

    Article  Google Scholar 

  12. M.J. Santofimia, L. Zhao, J. Sietsma: Metall. Mater. Trans. A, 2009, vol. 40, pp. 46-57.

    Article  Google Scholar 

  13. M.J. Santofimia, L. Zhao, R. Petrov, J. Sietsma: Mater. Charact., 2008, vol. 59, pp. 1758-1764.

    Article  Google Scholar 

  14. S.M.C. Van Bohemen, M.J. Santofimia, J. Sietsma: Scripta Mater., 2008, vol. 58, pp. 488-491.

    Article  Google Scholar 

  15. M.J. Santofimia, T. Nguyen-Minh, L. Zhao, R. Petrov, I. Sabirov, J. Sietsma: Mater. Sci. Eng. A, 2010, vol. 527, pp. 6429-6439.

    Article  Google Scholar 

  16. P. Kolmskog, A. Borgenstam, M. Hillert, P. Hedström, S.S. Babu, H. Terasaki, Y.-I. Komizo: Metall. Mater. Trans. A, 2012, vol. 43, pp. 4984-4988.

    Article  Google Scholar 

  17. S. Samanta, S. Das, D. Chakrabarti, I. Samajdar, S.B. Singh, A. Haldar: Metall. Mater. Trans. A, 2013, vol. 44, pp. 5653-5664.

    Article  Google Scholar 

  18. E.P. Da Silva, W. Xu, C. Föjer, Y. Houbaert, J. Sietsma, R.H. Petrov: Mater. Charact., 2014, vol. 95, pp. 85-93.

    Article  Google Scholar 

  19. E. Da Silva, D. De Knijf, W. Xu, C. Föjer, Y. Houbaert, J. Sietsma, R. Petrov: Mater. Sci. Technol., 2015, vol. 31, pp. 808-816.

    Article  Google Scholar 

  20. M.C. Somani, D.A. Porter, L.P. Karjalainen, R.D.K. Misra: Metall. Mater. Trans. A, 2014, vol. 45, pp. 1247-1257.

    Article  Google Scholar 

  21. A. Navarro-López, J. Sietsma, M.J. Santofimia: Metall. Mater. Trans. A, 2016, vol. 47, pp. 1028-1039.

    Article  Google Scholar 

  22. S. Samanta, P. Biswas, S. Giri, S.B. Singh, S. Kundu: Acta Mater., 2016, vol. 105, pp. 390-403.

    Article  Google Scholar 

  23. H. Beladi, I.B. Timokhina, X.-Y. Xiong, P.D. Hodgson: Acta Mater., 2013, vol. 61, pp. 7240-7250.

    Article  Google Scholar 

  24. I.B. Timokhina, K.D. Liss, D. Raabe, K. Rakha, H. Beladi, X.Y. Xiong, P.D. Hodgson: J. Appl. Cryst., 2016, vol. 49, pp. 399-414.

    Article  Google Scholar 

  25. T. Hilditch, H. Beladi, P.D. Hodgson, N. Stanford: Mater. Sci. Eng. A, 2012, vol. 534, pp. 288-296.

    Article  Google Scholar 

  26. ASTM E975-13: Standard Practice for X-ray Determination of Retained Austenite in Steel with Near Random Crystallographic Orientation, ASTM International, United States, 2013.

  27. A.K. De, J.G. Speer, D.K. Matlock, D.C. Murdock, M.C. Mataya, R.J. Comstock Jr: Metall. Mater. Trans. A, 2006, vol. 37, pp. 1875-1886.

    Article  Google Scholar 

  28. B.D. Cullity, J.W. Weymouth: Am. J. Phys., 1957, vol. 25, pp. 394-395.

    Article  Google Scholar 

  29. N.H. Van Dijk, A.M. Butt, L. Zhao, J. Sietsma, S.E. Offerman, J.P. Wright, S. Van der Zwaag: Acta Mater., 2005, vol. 53, pp. 5439-5447.

    Article  Google Scholar 

  30. J.H. Hollomon: Trans. AIME, 1945, vol. 162, pp. 268-290.

    Google Scholar 

  31. D.A. Korzekwa, D.K. Matlock, G. Krauss: Metall. Mater. Trans. A, 1984, vol. 15, pp. 1221.

    Article  Google Scholar 

  32. D.P. Koistinen, R.E. Marburger: Acta Metall., 1959, vol. 7, pp. 59-60.

    Article  Google Scholar 

  33. Y.J. Li, P. Choi, C. Borchers, S. Westerkamp, S. Goto, D. Raabe, R. Kirchheim: Acta Mater., 2011, vol. 59, pp. 3965-3977.

    Article  Google Scholar 

  34. H. Kong, Q. Chao, M.H. Cai, E.J. Pavlina, B. Rolfe, P.D. Hodgson, H. Beladi: Mater. Sci. Eng. A, 2017, vol. 707, pp. 538-547.

    Article  Google Scholar 

  35. F.Y. Wang,Y.F. Zhu, H.H. Zhou, B.Z. Jiang, G. Wang: Sci. China Technol. Sci.,2013, vol. 56, pp. 1847–1857.

    Article  Google Scholar 

  36. F. HajyAkbary, J. Sietsma, G. Miyamoto, T. Furuhara, M.J. Santofimia: Acta Mater., 2016, vol. 104, pp. 72-83.

    Article  Google Scholar 

  37. E.J. Seo, L. Cho, B.C. De Cooman: Acta Mater., 2016, vol. 107, pp. 354-365.

    Article  Google Scholar 

  38. F.G. Caballero, C. Garcia-Mateo, M.J. Santofimia, M.K. Miller, C.G. De Andres: Acta Mater., 2009, vol. 57, pp. 8-17.

    Article  Google Scholar 

  39. J. Sun, H. Yu, S. Wang, Y. Fan: Mater. Sci. Eng. A, 2014, vol. 596, pp. 89-97.

    Article  Google Scholar 

  40. C. Song, H. Yu, L. Li, T. Zhou, J. Lu, X. Liu: Mater. Sci. Eng. A, 2016, vol. 670, pp. 326-334.

    Article  Google Scholar 

  41. J. Zhang, H. Ding, R.D.K. Misra: Mater. Sci. Eng. A, 2015, vol. 636, pp. 53-59.

    Article  Google Scholar 

  42. L. Cho, E.J. Seo, B.C. De Cooman: Scripta Mater., 2016, vol. 123, pp. 69-72.

    Article  Google Scholar 

  43. H.K.D.H. Bhadeshia: Metal Sci., 1982, vol. 16, pp. 159-166.

    Article  Google Scholar 

  44. F.G. Caballero, M.J. Santofimia, C. Capdevila, C. García-Mateo, C. García de Andrés: ISIJ Int., 2006, vol. 46, pp. 1479-1488.

    Article  Google Scholar 

  45. M. Peet, H.K.D.H. Bhadeshia: http://www.msm.cam.ac.uk/map/steel/programs/mucg83.html. Accessed 2 May 2014.

  46. H.K.D.H. Bhadeshia, I.O. Materials: Bainite in steels, Inst. of Metals, 1992.

  47. H.K.D.H. Bhadeshia, D.V. Edmonds: Acta Metall., 1980, vol. 28, pp. 1265-1273.

    Article  Google Scholar 

  48. X.C. Xiong, B. Chen, M.X. Huang, J.F. Wang, L. Wang: Scripta Mater., 2013, vol. 68, pp. 321-324.

    Article  Google Scholar 

  49. F.G. Caballero, M.K. Miller, A.J. Clarke, C. Garcia-Mateo: Scripta Mater., 2010, vol. 63, pp. 442-445.

    Article  Google Scholar 

  50. J. Sun, H. Yu: Mater. Sci. Eng. A, 2013, vol. 586, pp. 100-107.

    Article  Google Scholar 

  51. X.-D. Tan, Y.-B. Xu, D. Ponge, X.-L. Yang, Z.-P. Hu, F. Peng, X.-W. Ju, D. Wu, D. Raabe: Mater. Sci. Eng. A, 2016, vol. 656, pp. 200-215.

    Article  Google Scholar 

  52. H. Rastegari, A. Kermanpur, A. Najafizadeh: Mater. Sci. Eng. A, 2015, vol. 632, pp. 103-109.

    Article  Google Scholar 

  53. Q. Li, X. Huang, W. Huang: Mater. Sci. Eng. A, 2016, vol. 662, pp. 129-135.

    Article  Google Scholar 

  54. C.H. Young, H.K.D.H. Bhadeshia: Mater. Sci. Technol., 1994, vol. 10, pp. 209-214.

    Article  Google Scholar 

  55. J. Shi, X. Sun, M. Wang, W. Hui, H. Dong, W. Cao: Scripta Mater., 2010, vol. 63, pp. 815-818.

    Article  Google Scholar 

  56. S. Zhang, K.O. Findley: Acta Mater., 2013, vol. 61, pp. 1895-1903.

    Article  Google Scholar 

  57. A.S. Podder, I. Lonardelli, A. Molinari, H.K.D.H. Bhadeshia: Proc. R. Soc. A, 2011, vol. 467, pp. 3141-3156.

    Article  Google Scholar 

  58. I.B. Timokhina, P.D. Hodgson, E.V. Pereloma: Metall. Mater. Trans. A, 2004, vol. 35, pp. 2331-2341.

    Article  Google Scholar 

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Acknowledgments

Deakin University’s Advanced Characterization Facility is acknowledged for use of the EM and X-ray instruments. Financial support provided by the Australian Automotive Technology Cooperative Research Centre (AutoCRC) 2020 HDR scholarship is gratefully acknowledged.

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Correspondence to H. Beladi.

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Manuscript submitted November 7, 2017.

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Kong, H., Chao, Q., Cai, M.H. et al. Microstructure Evolution and Mechanical Behavior of a CMnSiAl TRIP Steel Subjected to Partial Austenitization Along with Quenching and Partitioning Treatment. Metall Mater Trans A 49, 1509–1519 (2018). https://doi.org/10.1007/s11661-018-4525-3

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  • DOI: https://doi.org/10.1007/s11661-018-4525-3

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